TSKgel Alpha column

极性有机溶剂相色谱柱 TSKgel Alpha

TSKgel Alpha 是一种基材为亲水性甲基丙烯酸酯的尺寸排阻色谱柱,主要用于分析可溶于极性有机溶剂的聚合物,例如纤维素衍生物、聚酰亚胺、十二烷基硫酸钠(含有10 mmol/L LiBr的 DMF溶剂),清洁凝胶(甲醇溶剂)、以及聚乙烯醇的皂化度(HFIP溶剂)等。图1是TSKgel Alpha 色谱柱的校准曲线。

图 1: TSKgel Alpha 色谱柱的校准曲线

与TSKgel PW 系列色谱柱不同的是,Alpha色谱柱可在100%极性有机溶剂流动相中使用。图2显示了此款色谱柱可以使用的溶剂

图 2: TSKgel Alpha-3000 色谱柱与有机溶剂的相容性

TSKgel Alpha-M 混合床柱
混合床柱TSKgel Alpha-M 的校准曲线直线范围广,适合用来分析分子量未知的聚合物样品或分子量分布比较宽的样品。

Base Material: hydrophilic methacylate
Particle Size (mean): 7 µm
Pore size (mean): 2.5 nm
Exclusion Limit (Polyethylene oxide - Water):   5,000 Da
Exclusion Limit (Polystyrene - THF): 10,000 Da
Shipping Solvent water
Max. Pressure Drop: 4 MPa  

P/N
Description
Particle size
Housing material ID (mm) Length (cm)
0018339
TSKgel Alpha-2500
7 µm
Stainless Steel 7.8 30
0018345
Guard Column for P/N 0018339
13 µm
Stainless Steel 6 4
Base Material: hydrophilic methacylate
Particle Size (mean): 7 µm
Pore size (mean): 15 nm
Exclusion Limit (Polyethylene oxide - water):   90,000 Da
Exclusion Limit (Polystyrene - THF): 100,000 Da
Shipping Solvent water
Max. Pressure Drop: 4 MPa  

P/N
Description
Particle size
Housing material ID (mm) Length (cm)
0018340
TSKgel Alpha-3000
7 µm
Stainless Steel 7.8 30
0018345
Guard Column for P/N 0018340
13 µm
Stainless Steel 6 4
Base Material: hydrophilic methacylate
Particle Size (mean): 10 µm 
Pore size (mean): 45 nm 
Exclusion Limit (Polyethylene oxide - water):   400,000 Da
Exclusion Limit (Polystyrene - THF): 1 million Da
Shipping Solvent water
Max. Pressure Drop: 3 MPa  

P/N
Description
Particle size
Housing material ID (mm) Length (cm)
0018341
TSKgel Alpha-4000
10 µm
Stainless Steel 7.8 30
0018345
Guard Column for P/N 0018341
13 µm
Stainless Steel 6 4
Base Material: hydrophilic methacylate
Particle Size (mean): 10 µm
Pore size (mean): 100 nm
Exclusion Limit (Polyethylene oxide - water):   1 million Da
Exclusion Limit (Polystyrene - THF): 7 million Da
Shipping Solvent water
Max. Pressure Drop: 3 MPa  

P/N
Description
Particle size
Housing material ID (mm) Length (cm)
0018342
TSKgel Alpha-5000
10 µm
Stainless Steel 7.8 30
0018345
Guard column for P/N 0018342
13 µm
Stainless Steel 6 4
Base Material: hydrophilic methacylate
Particle Size (mean): 13 µm
Pore size (mean): ND 
Exclusion Limit (Polyethylene oxide - water):   > 107 Da
Exclusion Limit (Polystyrene - THF): > 107 Da
Shipping Solvent water
Max. Pressure Drop: 2 MPa  

P/N
Description
Particle size
Housing material ID (mm) Length (cm)
0018343
TSKgel Alpha-6000
13 µm
Stainless Steel 7.8 30
0018345
Guard Column for P/N 0018343
13 µm
Stainless Steel 6 4
Base Material: hydrophilic methacylate
Particle Size (mean): 13 µm
Exclusion Limit (Polyethylene oxide - water):   > 107 Da
Exclusion Limit (Polystyrene - THF): > 107 Da
Shipping Solvent water
Max. Pressure Drop: 2 MPa  

P/N
Description
Particle size
Housing material ID (mm) Length (cm)
0018344
TSKgel Alpha-M
13 µm
Stainless Steel 7.8 30
0018345
Guard Column for P/N 0018344
13 µm
Stainless Steel 6 4